Experimental Assessment of a Laboratory Rotary Sample Splitter

Authors

  • Nenuwa, Olushola B Minerals & Petroleum Resources Engineering Department, Federal Polytechnic, P.M.B. 5351, Ado-Ekiti, Ekiti state, Nigeria.
  • Oke Olugbenga O Minerals & Petroleum Resources Engineering Department, Federal Polytechnic, P.M.B. 5351, Ado-Ekiti, Ekiti state, Nigeria.
  • Sanya Olajide T Glass & Ceramic Technology Department, Federal Polytechnic, P.M.B. 5351, Ado-Ekiti, Ekiti state, Nigeria.

Keywords:

Bias, Precision, Riffling, Sampling, Splitting, Subsampling

Abstract

A binary mixture of iron chips and sand was used to experimentally test the performance of a constructed laboratory sample splitter. Four tests were conducted and six subsamples were produced in each case. The subsamples were separated into their constituents and the percentage weight of iron chips was determined. The results obtained were examined statistically and it was observed that the mean value of the percentage weight of iron chips in the subsamples range from 30.4 – 35.7% which compared well with the sample true value of 33.3%. The biases of the subsamples range from 0.2 – 2.9%, the variance ranges from 0.790 – 2.334 while the coefficient of variation is 0.025 – 4.6%. The standard deviation of the subsamples produced in the experiment is 0.0889 – 1.5277%. The level of accuracy and precision of rotary sample riffling is superior to some other sampling techniques and the machine tested gave an intermediate performance indicating that it is suitable for routine and non-critical works. Rotary Sample Splitter is therefore recommended for splitting dry granular samples, whenever an efficient, accurate and mechanized technique for sample splitting is desired.

References

1. Allen, T. (1964): Silic. Indust. 29,12,409 - 15.
2. Allen T. (1996): Particle Size Measurement, Vol. 1, Chapman & Hall, London.
3. Allen T. (1981): Particle Size Measurement - Third Edition (Powder Technology Series). Chapman & Hall. Pp. 1 – 35.
4. Crumbling D.M. (2001): Applying the Concept of Effective Data to Environmental Analyses for Contaminated Sites, EPA 542-R-01-013, US Environmental Protection Agency,Washington, DC.
5. Gandhi S.M. and Sarkar B.C. (2016): Essentials of Mineral Exploration and Evaluation. Elsevier Inc. Pp. 235 – 255.
6. Gerlach, R.W., Nocerino, J.M., Ramsey, C.A., Venner, B. C. (2003):Gy sampling theory in environmental studies, Sampling error estimates. Elsevier. Pp. 159 – 168.
7. Gupta A. and Yan D.S. (2006): Mineral Processing Design and Operation: An Introduction. Elsevier B.V. pp. 1 – 31.
8. Gy P. (1979): Sampling of Particulate Material: Theory and Practice, Elsevier Scientific Publishing Co., Amsterdam.
9. Gy P. (1998): Sampling for Analytical Purposes. Wiley, New York.
10. Hawes, R.W.M. and Muller, L.D. (1960): A Small Rotary Sampler and Preliminary Study of its Use, AERE - R - 3051, Harwell, Oxfordshire, England.
11. Holmes, R.J. (1991): Sampling methods: Problems and solutions, in Evaluation and Optimization of Metallurgical Performance, ed. D. Malhotra et al., SME Inc., Littleton, Chapter 16.
12. Ingamells, C.O. and Pitard, F.F. (1986): Applied Geochemical Analyses. J. Wiley and Sons, Inc. New York. 733 pp.
13. Jenkins T.F., Grant C.L., Brar G.S., Thorne P.G., Schumacher P.W., Ranney T.A. (1997): Field Anal. Chem. Technol. 1 (3)151–163.
14. Khan (1968): Thesis, Bradford University.
15. Myers J.C. (1997):Geostatistical Error Management: Quantifying Uncertainty for Environmental Sampling and Mapping. Van Nostrand Reinhold, New York.
16. Pitard F.F. (1993): Pierre Gy’s Sampling Theory and Sampling Practice (2nd Edition). CRC Press: Boca Raton, FL.
17. Pownall, J.H. (1959): The Construction and Testingofa Large Laboratory Rotary Sampling Machine, AERE - R - 2861, Harwell, Oxfordshire, England.
18. Smith P.L. (2001): A Primer for Sampling Solids, Liquids, and Gases,Society for Industrial and Applied Mathematics, Philadelphia, PA.
19. Taggart (1945): Handbook of Mineral Dressing. Wiley, Section 19.
20. Wentworth, C.K., Wilgers, W.L. and Koch, H.L. (1934): A rotary type of sample divider. J. Sed. Pet., 4, 127.
21. Wills, B.A. (2006): Will’s Mineral Processing Technology: An introduction to the practical aspects of ore treatment and mineral recovery, 7th edition, Elsevier Ltd, pg. 40.

Published

2018-06-28